2-氨基-3-氰基-N-苄基吡咯合成路线 (共 7 条)
反应条件
hydrogen; palladium on activated charcoal in methanol T=20°C; P=2068.59 Torr; 1.5 h;
参考文献
Chien, Tun-Cheng; Meade, Eric A.; Hinkley, Jack M.; Townsend, Leroy B.
Organic Letters, 2004 , vol. 6, # 17 p. 2857 - 2859
反应条件
potassium hydroxide in ethylene glycol T=110 - 115°C; 1.5 h;
参考文献
Chien, Tun-Cheng; Meade, Eric A.; Hinkley, Jack M.; Townsend, Leroy B.
Organic Letters, 2004 , vol. 6, # 17 p. 2857 - 2859
反应条件
1: diphenylphosphoryl azide; Et3N / dimethylformamide / 6 h / 20 °C 2: 4.695 g / dimethylformamide; methanol / 8 h / 65 °C 3: 59 percent / KOH / ethane-1,2-diol / 1.5 h / 110 - 115 °C View Scheme
参考文献
Organic Letters, , vol. 6, # 17 p. 2857 - 2859
反应条件
1: 4.695 g / dimethylformamide; methanol / 8 h / 65 °C 2: 59 percent / KOH / ethane-1,2-diol / 1.5 h / 110 - 115 °C View Scheme
参考文献
Organic Letters, , vol. 6, # 17 p. 2857 - 2859
反应条件
toluene-4-sulfonic acid in dichloromethane T=20°C; 24 h;
参考文献
Chien, Tun-Cheng; Meade, Eric A.; Hinkley, Jack M.; Townsend, Leroy B.
Organic Letters, 2004 , vol. 6, # 17 p. 2857 - 2859
反应条件
1.1: benzene / 2 h / Heating 1.2: NaBH4 / ethanol / 24 h / 20 °C 2.1: 1.37 g / p-TsOH*H2O / CH2Cl2 / 24 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 6, # 17 p. 2857 - 2859
反应条件
1: With tetra(n-butyl)ammonium hydrogensulfate in acetonitrile 3 h; Heating; 2: With ammonia in methanol T=60°C; 4 h;
参考文献
Chien, Tun-Cheng; Meade, Eric A.; Hinkley, Jack M.; Townsend, Leroy B.
Organic Letters, 2004 , vol. 6, # 17 p. 2857 - 2859