反应条件
1: vinylidene difluoride With sec.-butyllithium in tetrahydrofuran
T=-105 - -70°C;
2: triisopropylsilyl chloride With N,N,N',N',N'',N''-hexamethylphosphoric triamide in tetrahydrofuran
参考文献
Hanamoto, Takeshi; Koga, Yukinori; Kawanami, Toshio; Furuno, Hiroshi; Inanaga, Junji
Angewandte Chemie - International Edition, 2004 , vol. 43, # 27 p. 3582 - 3584
