2-氰基吡啶-3-甲酸甲酯合成路线 （共 13 条）
反应条件
pyridine in methanol
参考文献
Spiessens, Luc I. M.; Anteunis, Marc J. O.
Bulletin des Societes Chimiques Belges, 1980 , vol. 89, # 3 p. 205 - 232
反应条件
chloroformic acid ethyl ester; triethylamine
参考文献
Spiessens, Luc I. M.; Anteunis, Marc J. O.
Bulletin des Societes Chimiques Belges, 1980 , vol. 89, # 3 p. 205 - 232
反应条件
1: 25 percent / Ac2O / pyridine 2: 31 percent / pyridine / methanol View Scheme
参考文献
Bulletin des Societes Chimiques Belges, , vol. 89, # 3 p. 205 - 232
反应条件
in acetonitrile T=27°C; Yield given. Yields of byproduct given;
参考文献
Heterocycles, , vol. 22, # 5 p. 1121 - 1124
反应条件
in acetonitrile T=27°C; Yield given. Yields of byproduct given;
参考文献
Heterocycles, , vol. 22, # 5 p. 1121 - 1124
反应条件
1: SOCl2 View Scheme
参考文献
Helvetica Chimica Acta, , vol. 34, p. 488,489
参考文献
Helvetica Chimica Acta, , vol. 34, p. 488,489
参考文献
Helvetica Chimica Acta, , vol. 34, p. 488,489
反应条件
N,N-dimethylcarbamoyl chloride in dichloromethane Ambient temperatureother 3-substituted pyridine 1-oxides, var. temps.; Product distributionMechanism;
参考文献
Heterocycles, , vol. 22, # 1 p. 93 - 96
反应条件
1: 93 percent / H2, conc. hydrochloric acid / 10percent Pd/C / methanol / 3 h / 760 Torr / Ambient temperature 2: 76 percent / 4 h / 20 - 35 °C 3: 66 percent / LiAlH4, diethylamine / pentane / 1 h / Ambient temperature View Scheme
参考文献
Fos; Bosca; Mauleon; Carganico
Journal of Heterocyclic Chemistry, 1993 , vol. 30, # 2 p. 473 - 476
