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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
75366-04-0
合成路线
（共 7 条）
75366-04-0
→
反应条件
620-19-9
3-甲基苄基氯
+
552-45-4
邻甲基氯化苄
反应条件
hydrogenchloride in tetrachloromethane 1 h; reaction regioselectivity; a series of reagents; Product distributionMechanism;
参考文献
Bee, Lim Keow; Garratt, Peter J.; Mansuri, Muzamil M.
Journal of the American Chemical Society, 1980 , vol. 102, # 23 p. 7076 - 7079
75366-04-0
→
反应条件
576-22-7
2-溴-1,3-二甲苯
+
576-23-8
2,3-二甲基溴苯
反应条件
bromine; tri-n-butyl-tin hydride multistep reaction; reaction regioselectivity; a series of reagents; Product distributionMechanism;
参考文献
Journal of the American Chemical Society, , vol. 102, # 23 p. 7076 - 7079
75366-04-0
→
反应条件
576-22-7
2-溴-1,3-二甲苯
+
576-23-8
2,3-二甲基溴苯
反应条件
bromine; tri-n-butyl-tin hydride multistep reaction; reaction regioselectivity; a series of reagents; Product distributionMechanism;
参考文献
Bee, Lim Keow; Garratt, Peter J.; Mansuri, Muzamil M.
Journal of the American Chemical Society, 1980 , vol. 102, # 23 p. 7076 - 7079
75366-04-0
→
反应条件
620-19-9
3-甲基苄基氯
+
552-45-4
邻甲基氯化苄
反应条件
hydrogenchloride in tetrachloromethane 1 h; reaction regioselectivity; a series of reagents; Product distributionMechanism;
参考文献
Bee, Lim Keow; Garratt, Peter J.; Mansuri, Muzamil M.
Journal of the American Chemical Society, 1980 , vol. 102, # 23 p. 7076 - 7079
75366-04-0
→
反应条件
66790-58-7
3-甲基-2-溴苄溴
+
75366-10-8
反应条件
bromine in tetrachloromethane T=-10°C; 0.5 h; reaction regioselectivity; a series of reagents; Product distributionMechanism;
参考文献
Bee, Lim Keow; Garratt, Peter J.; Mansuri, Muzamil M.
Journal of the American Chemical Society, 1980 , vol. 102, # 23 p. 7076 - 7079
4794-04-1
1,4-二氢苯甲酸
→
反应条件
75366-04-0
反应条件
<b>Multi-step reaction with 5 steps<br /> </b>1: LiAlH<sub>4</sub> <br />3: LiAlH<sub>4</sub> <br />4: 40 percent / KO-t-Bu / pentane / 1.) -20 deg C, 2 h, room temperature, 14 h<br />5: 27 percent / KO-t-Bu / dimethylsulfoxide / 0.5 h<br /> <br />
参考文献
Bee, Lim Keow; Garratt, Peter J.; Mansuri, Muzamil M. Journal of the American Chemical Society, 1980 , vol. 102, # 23 p. 7076 - 7079
534-22-5
2-甲基呋喃
→
反应条件
75366-04-0
反应条件
<b>Multi-step reaction with 2 steps<br /> </b>1: 56 percent / 2 h / -20 °C<br />2: 30 percent / LiAlH<sub>4</sub>, TiCl<sub>3</sub> / tetrahydrofuran / 20 h<br /> <br />
参考文献
Mueller, Paul; Schaller, Jean-Pierre Helvetica Chimica Acta, 1989 , vol. 72, p. 1608 - 1617
