in dichloromethane (OC)5ReFBF3 is suspended in CH2Cl2 under N2, addn. of trimethylvinylsilane, mixture is stirred for 72 h at room temp.; yellow soln. and colourless ppt. are obained, sepn. of ppt. and drying under vac., elem. anal.;
参考文献
Steil, Peter; Beck, Wolfgang; Stone, F. Gordon A.
Journal of Organometallic Chemistry, 1989 , vol. 368, p. 77 - 82