1: With [Ir(μ-Cl)(cyclooctene)2]2 in dichloromethane
T=20°C; 0.5 h;
2: With hydrogenchloride in 1,4-dioxane; dichloromethane
0.5 h; regioselective reaction;
参考文献
Park, Jung-Woo; Park, Sung Joon; Jun, Chul-Ho
Organic Letters, 2012 , vol. 14, # 6 p. 1468 - 1471
AlEt1.5Cl1.5; triphenylphosphine; nickel dichloride
T=100°C; 8 h; Further byproducts given. Yields of byproduct given;
参考文献
Gailyunas, G. A.; Nurtdinova, G. V.; Yusupova, F. G.; Khalilov, L. M.; Mavrodiev, V. K.; et al.
Journal of Organometallic Chemistry, 1981 , vol. 209, # 2 p. 139 - 146
bis(1,5-cyclooctadiene)nickel (0); diethylaluminium chloride; triphenylphosphine in toluene
T=50°C; 48 h; other ligands, var. P/Ni and Al/Ni ratios, var. reaction times; Product distribution;
参考文献
Cros, Philippe; Triantaphylides, Christian; Buono, Gerard
Journal of Organic Chemistry, 1988 , vol. 53, # 1 p. 185 - 187
