(S)-(-)-β-香茅醇合成路线 (共 44 条)
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Mori, Kenji; Ohtaki, Takashi; Ohrui, Hiroshi; Berkebile, Dennis R.; Carlson, David A.
Bioscience, Biotechnology and Biochemistry, 2004 , vol. 68, # 8 p. 1768 - 1778
反应条件
lt;lt;(-)-2,2'-bis(diphenylphosphino)-4,4',6,6'-tetramethyl-3,3'-bibenzolt;bgt;thiophenegt;Ru(p-cumene)Igt;I; hydrogen in methanol T=25°C; P=7355.08 Torr; 88 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 61, # 18 p. 6244 - 6251
反应条件
bis(norbornadiene)rhodium(I) tetrafluoroborate; (RC,SFc,SP)-ChenPhos; hydrogen in dichloromethane T=20°C; P=19001.3 Torr; 20 h; Inert atmosphereAutoclave; enantioselective reaction;
参考文献
Wang, Quanjun; Liu, Xueying; Liu, Xian; Li, Bin; Nie, Huifang; Zhang, Shengyong; Chen, Weiping
Chemical Communications, 2014 , vol. 50, # 8 p. 978 - 980
反应条件
hydrogen; [Ru(p-cymene)I-(S)-binap]I in methanol; water T=20°C; P=76000 Torr; 8 h; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 59, # 11 p. 3064 - 3076
反应条件
ammonia; lithium in tetrahydrofuran T=-30°C; 0.666667 h;
参考文献
Mori, Kenji; Sugai, Takeshi
Synthesis, 1982 , # 9 p. 752 - 753
反应条件
sodium hydroxide in methanol Ambient temperature;
参考文献
Hirama, Masahiro; Noda, Takeshi; Ito, Sho
Journal of Organic Chemistry, 1985 , vol. 50, # 1 p. 127 - 129
反应条件
(S)-p-Tol-BINAP; potassium hydroxide T=100°C; 2 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Wu, Ruoqiu; Beauchamps, Marie G.; Laquidara, Joseph M.; Sowa Jr., John R.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 9 p. 2106 - 2110
反应条件
{[(S)-2,2'-di((p-tolyl)2P)-1,1'-binaphthyl]RuCl2}2*NEt3; hydrogen in methanol T=19.9°C; P=3750.3 Torr; Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 117, # 50 p. 12647 - 12648
反应条件
hydrogen; lt;(+)-CyBINAPgt;-RhN in benzene P=15200 Torr; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Chemistry Letters, , p. 1007 - 1008
反应条件
Fusarium concentricum in dimethyl sulfoxide T=28 - 30°C; 120 h; Microbiological reaction; Reagent/catalyst;
参考文献
Chemistry and Biodiversity, , vol. 10, # 10 p. 1909 - 1919