(9CI)-5,6,7,8-四氢-8-(1-甲基乙基)-喹啉合成路线 (共 9 条)
反应条件
nitrobenzene; palladium on activated charcoal in xylene
Heating;
参考文献
Hoenel, Michael; Vierhapper, Friedrich W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1933 - 1939
反应条件
hydrogen; platinum(IV) oxide in trifluoroacetic acid
参考文献
Hoenel, Michael; Vierhapper, Friedrich W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1933 - 1939
反应条件
1: 47 percent / toluene-p-sulphonic acid / toluene / Heating
2: 80 percent / ethanol / 36 h / Heating
3: LiAlH4 / diethyl ether
5: 16 percent / nitrobenzene / 10percent palladium on C / xylene / Heating
6: 70 percent / hydrogen / platinum oxide / trifluoroacetic acid
View Scheme
参考文献
Hoenel, Michael; Vierhapper, Friedrich W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1933 - 1939
反应条件
1: 80 percent / ethanol / 36 h / Heating
2: LiAlH4 / diethyl ether
4: 16 percent / nitrobenzene / 10percent palladium on C / xylene / Heating
5: 70 percent / hydrogen / platinum oxide / trifluoroacetic acid
View Scheme
参考文献
Hoenel, Michael; Vierhapper, Friedrich W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1933 - 1939
反应条件
2: 16 percent / nitrobenzene / 10percent palladium on C / xylene / Heating
3: 70 percent / hydrogen / platinum oxide / trifluoroacetic acid
View Scheme
参考文献
Hoenel, Michael; Vierhapper, Friedrich W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1933 - 1939
反应条件
1: LiAlH4 / diethyl ether
3: 16 percent / nitrobenzene / 10percent palladium on C / xylene / Heating
4: 70 percent / hydrogen / platinum oxide / trifluoroacetic acid
View Scheme
参考文献
Hoenel, Michael; Vierhapper, Friedrich W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1933 - 1939
反应条件
1: 101.5 g / hydrazine hydrate / Raney nickel / ethanol / 2 h / Heating
2: 56 percent / As2O5, conc. H2SO4 / Heating
3: 70 percent / hydrogen / platinum oxide / trifluoroacetic acid
View Scheme
参考文献
Hoenel, Michael; Vierhapper, Friedrich W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1933 - 1939
反应条件
1: 16 percent / nitrobenzene / 10percent palladium on C / xylene / Heating
2: 70 percent / hydrogen / platinum oxide / trifluoroacetic acid
View Scheme
参考文献
Hoenel, Michael; Vierhapper, Friedrich W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1933 - 1939
反应条件
1: 56 percent / As2O5, conc. H2SO4 / Heating
2: 70 percent / hydrogen / platinum oxide / trifluoroacetic acid
View Scheme
参考文献
Hoenel, Michael; Vierhapper, Friedrich W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1933 - 1939