4-(5,6,7,8-四氢萘-1-基)丁酸合成路线 （共 10 条）
反应条件
potassium hydroxide in water; ethylene glycol
Heating;
参考文献
Isabelle, M. Elaine; Wightman, Robert H.; Avdovich, Hajro W.; Laycock, David E.
Canadian Journal of Chemistry, 1980 , vol. 58, p. 1344 - 1349
反应条件
2: 90 percent / lithium aluminum hydride / diethyl ether / 24 h / Ambient temperature
3: 90 percent / phosphorus tribromide / benzene
4: 90 percent / methanol / Heating
5: 85 percent / potassium hydroxide / H2O; ethane-1,2-diol / Heating
View Scheme
参考文献
Isabelle, M. Elaine; Wightman, Robert H.; Avdovich, Hajro W.; Laycock, David E.
Canadian Journal of Chemistry, 1980 , vol. 58, p. 1344 - 1349
反应条件
1: 90 percent / methanol / Heating
2: 85 percent / potassium hydroxide / H2O; ethane-1,2-diol / Heating
View Scheme
参考文献
Isabelle, M. Elaine; Wightman, Robert H.; Avdovich, Hajro W.; Laycock, David E.
Canadian Journal of Chemistry, 1980 , vol. 58, p. 1344 - 1349
反应条件
1: 90 percent / phosphorus tribromide / benzene
2: 90 percent / methanol / Heating
3: 85 percent / potassium hydroxide / H2O; ethane-1,2-diol / Heating
View Scheme
参考文献
Isabelle, M. Elaine; Wightman, Robert H.; Avdovich, Hajro W.; Laycock, David E.
Canadian Journal of Chemistry, 1980 , vol. 58, p. 1344 - 1349
反应条件
1: 90 percent / lithium aluminum hydride / diethyl ether / 24 h / Ambient temperature
2: 90 percent / phosphorus tribromide / benzene
3: 90 percent / methanol / Heating
4: 85 percent / potassium hydroxide / H2O; ethane-1,2-diol / Heating
View Scheme
参考文献
Isabelle, M. Elaine; Wightman, Robert H.; Avdovich, Hajro W.; Laycock, David E.
Canadian Journal of Chemistry, 1980 , vol. 58, p. 1344 - 1349
反应条件
hydrogenchloride; amalgamated zinc
Einleiten von Chlorwasserstoff;
参考文献
Schroeter
Chemische Berichte, 1924 , vol. 57, p. 2014
Chem. Zentralbl., 1928 , vol. 99, # II p. 1386
反应条件
aluminium trichloride; chlorobenzene
Erhitzen des Reaktionsprodukts mit wss. Bromwasserstoffsaeure, Erwaermen der gebildeten Bromide mit Malonsaeure-diaethylester und Natriumaethylat in Aethanol. Erhitzen auf 220grad;
参考文献
Colonge; Rochas
Bulletin de la Societe Chimique de France, 1948 , p. 827
参考文献
Schroeter
Chemische Berichte, 1924 , vol. 57, p. 2014
Chem. Zentralbl., 1928 , vol. 99, # II p. 1386
反应条件
phosphorus pentachloride
nachfolgend Destillation unter vermindertem Druck;
参考文献
Isabelle, M. Elaine; Wightman, Robert H.; Avdovich, Hajro W.; Laycock, David E.
Canadian Journal of Chemistry, 1980 , vol. 58, p. 1344 - 1349
反应条件
nachfolgend Destillation unter vermindertem Druck;
参考文献
Schroeter
Chemische Berichte, 1924 , vol. 57, p. 2014
Chem. Zentralbl., 1928 , vol. 99, # II p. 1386
Show Details
Riedel,J. D.
Patent: DE397150 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 461
