2-氨基-1-(3-氨基苯基)乙醇合成路线 (共 2 条)
反应条件
1: sodium azide / dichloromethane / 8 h / 20 - 70 °C / Inert atmosphere
2: palladium 10 on activated carbon; hydrogen / methanol / 5 h / 20 °C / Inert atmosphere
View Scheme
参考文献
Heller, Stephen T.; Schultz, Erica E.; Sarpong, Richmond
Angewandte Chemie - International Edition, 2012 , vol. 51, # 33 p. 8304 - 8308
反应条件
1: sodium tetrahydroborate / Inert atmosphere
2: sodium azide / dichloromethane / 8 h / 20 - 70 °C / Inert atmosphere
3: palladium 10 on activated carbon; hydrogen / methanol / 5 h / 20 °C / Inert atmosphere
View Scheme
参考文献
Heller, Stephen T.; Schultz, Erica E.; Sarpong, Richmond
Angewandte Chemie - International Edition, 2012 , vol. 51, # 33 p. 8304 - 8308