2,3-二甲基-5-(2-甲基丁基)吡嗪合成路线 (共 2 条)
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II) in tetrahydrofuran
T=20°C; Negishi coupling reaction; 12 h; Inert atmosphere;
参考文献
Pitchaiah, Arigala; Hwang, Intaek; Hwang, Jin-Soo; Kim, Hyungrok; Lee, Kee-In
Synthesis (Germany), 2012 , vol. 44, # 11 art. no. SS-2012-F0234-OP, p. 1631 - 1636
反应条件
1: pyridine / chloroform / 2.5 h / -78 - 20 °C / Inert atmosphere
2: [1,3-bis(diphenylphosphino) propane] dichloronickel(II) / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere
View Scheme
参考文献
Pitchaiah, Arigala; Hwang, Intaek; Hwang, Jin-Soo; Kim, Hyungrok; Lee, Kee-In
Synthesis (Germany), 2012 , vol. 44, # 11 art. no. SS-2012-F0234-OP, p. 1631 - 1636