反应条件
1: 1.) n-BuLi, 2.) I2 / 1.) petroleum ether, hexane, 1 h, 2.) petroleum ether, hexane, 40 min
2: 1.) 10percent aq. KOH, 2.) HONH2*HCl, CuCl, EtNH2, 4.) 2N aq. H2SO4
3: oxalyl chloride / 72 h / Ambient temperature
View Scheme
参考文献
Holtzapple, Mark T.; VanDuker, Frank C.; Nam, Ki Y.; Lalond, James J.
Organic Preparations and Procedures International, 1995 , vol. 27, # 4 p. 507 - 510
