反应条件
(C5H4N)2 in tetrahydrofuran byproducts: (CH3CH2)3GeCl; (dry Ar); soln. of (Et3Ge)2Cd added to TiCl4*2THF at -20°C; 1 h;after 20 h at 20°C Cd and TiCl3*3THF pptd.; bipy added to THF soln., kept for 24 h at 20°C, TiCl1.7*1.5bipy pptd.; THF removed in vacuo, residue washed (hexane), dried; elem. anal.;
参考文献
Russian Chemical Bulletin, , vol. 43, # 7 p. 1242 - 1244
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 7 p. 1305 - 1307
