Solomakhina, F. Kh.
Tr. Tashkent. Farm. Inst., 1960 , vol. 2, p. 317 - 325
C.A., 1962 , vol. 57, p. 11230
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Gmelin Handbook: Bi: Org.Verb., 1.3.3.2.4.3, page 72 - 78
Gmelin Handbook: Cl: SVol.B2, 123, page 577 - 578
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Fink, W.
Diss. Muenchen 1957, S. 18
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Fink, W.
Diss. Muenchen 1957, S. 52
in neat (no solvent) byproducts: NaCl; solid-liquid metathesis reaction of starting materials at room temp. under N2; trituration with water or MeOH to remove NaCl, SEM, EDXA;
参考文献
Hector, Andrew L.; Parkin, Ivan P.
Inorganic Chemistry, 1994 , vol. 33, p. 1727 - 1728
NH4I-NH3 in tetrachloromethane soln. of TiCl4 added to alcohol with cooling and stirring, soln. added to NH4I-NH3 with stirring and cooling at 0-15°C; organic layer separated, solvent removed, product distilled under vacuum;
参考文献
Yatluk; Suvorov
Journal of applied chemistry of the USSR, 1985 , vol. 58, # 8 pt 2 p. 1678 - 1680
in chloroform-d1 react. of Cy3SnCH2CHCHCH3 with TiCl4 (1 equiv) at 30°C under complete and rapid formation of Cy3SnCl and a brown ppt. of the allyl titanium trichloride;
