反应条件
in neat (no solvent) TiCl4 was slowly added to tetraisopropoxytitanium at 0°C, then the mixt. allowed to warm up to room temp.;; distn. (61-65°C/0.1 Torr), the purity of the product exceeds 98 percent, it solidified at room temp., but could be easily liquified to handle;;
参考文献
Reetz, Manfred T.; Westermann, Juergen; Steinbach, Rainer; Wenderoth, Bernd; Peter, Roland; et al.
Chemische Berichte, 1985 , vol. 118, # 4 p. 1421 - 1440
