反应条件
in tetrahydrofuran byproducts: LiCl; N2-atmosphere; slow addn. of excess of Li-salt to TiCl4 at -78°C,stirring (room temp., overnight); evapn. (reduced pressure), extn. into MePh, filtration off of LiCl, concn., crystn. (-20°C, overnight), filtration, washing (MePh, 0°C), drying (vac.); elem. anal.;
参考文献
Polo, Eleonora; Bellabarba, Ronan M.; Prini, Giansiro; Traverso, Orazio; Green, Malcolm L.H.
Journal of Organometallic Chemistry, 1999 , vol. 577, # 2 p. 211 - 218
