反应条件
in toluene
Dropwise addn. of TiCl4 in toluene to soln. of C(CH3)5Si(CH3)3 in toluene (N2), stirring (2 h, color change from red-orange to red).; Evapn. of solvent and byproduct (vacuum), washing of crystals (pentane), dried (vacuum), elem. anal.;
参考文献
Llinas, Gerardo Hidalgo; Mena, Miguel; Palacios, Federico; Royo, Pascual; Serrano, Ricardo
Journal of Organometallic Chemistry, 1988 , vol. 340, p. 37 - 40
