meta-chloroperoxybenzoic acid; tri-n-butyl-tin hydride in methanol; dichloromethane; water T=10°C; dark;
参考文献
Murakami, Yukito; Hisaeda, Yoshio; Kikuchi, Jun-ichi; Ohno, Teruhisa; Suzuki, Masashi; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 1237 - 1246
→
反应条件
in N,N-dimethyl-formamide Electrolysis; controlled-potential electrolysis at -1.5 V vs. SCE in DMF containing Bu4NF and AcOH at 20.5°C in the dark; not isolated; the reaction was monitored by electronic spectroscopy, ESR spin-trapping technique;
参考文献
Murakami, Yukito; Hisaeda, Yoshio; Ozaki, Toshiaki; Tashiro, Takako; Ohno, Teruhisa; et al.
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 1 p. 311 - 324
sodium hydride in N,N-dimethyl-formamide; benzene
2 h; Ambient temperature;
参考文献
Murakami, Yukito; Hisaeda, Yoshio; Ozaki, Toshiaki; Tashiro, Takako; Ohno, Teruhisa; et al.
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 1 p. 311 - 324