2-苯基苯并[cd]吲哚-5(1h)-酮合成路线 （共 7 条）
反应条件
potassium hydroxide in methanol; water
3 h; Heating;
参考文献
Neidlein, Richard; Moller, Franz
Liebigs Annalen der Chemie, 1980 , # 6 p. 971 - 979
反应条件
1: 44 percent / pyridine / 12 h / Ambient temperature
2: 13 percent / ester of polyphosphoric acid / 0.33 h / Heating
3: 50 percent / KOH / methanol; H2O / 3 h / Heating
View Scheme
参考文献
Neidlein, Richard; Moller, Franz
Liebigs Annalen der Chemie, 1980 , # 6 p. 971 - 979
反应条件
1: 13 percent / ester of polyphosphoric acid / 0.33 h / Heating
2: 50 percent / KOH / methanol; H2O / 3 h / Heating
View Scheme
参考文献
Neidlein, Richard; Moller, Franz
Liebigs Annalen der Chemie, 1980 , # 6 p. 971 - 979
反应条件
1: 44 percent / pyridine / 12 h / Ambient temperature
2: 13 percent / ester of polyphosphoric acid / 0.33 h / Heating
3: 50 percent / KOH / methanol; H2O / 3 h / Heating
View Scheme
参考文献
Neidlein, Richard; Moller, Franz
Liebigs Annalen der Chemie, 1980 , # 6 p. 971 - 979
反应条件
PPA
T=75 - 80°C; 15 h; Yields of byproduct given;
参考文献
Neidlein; Moller
Archiv der Pharmazie, 1980 , vol. 313, # 12 p. 977 - 984
反应条件
potassium hydroxide; PPA
1.) 75 to 80 deg C, 15 h, 2.) aq. methanol, reflux, 3 h; Yield given. Multistep reaction;
参考文献
Neidlein; Moller
Archiv der Pharmazie, 1980 , vol. 313, # 12 p. 977 - 984
反应条件
potassium carbonate in acetone
12 h; Ambient temperature;
参考文献
Neidlein, Richard; Moller, Franz
Liebigs Annalen der Chemie, 1980 , # 6 p. 971 - 979
