反应条件
in dichloromethane-d2 Sonication; in situ; under N2 or Ar atm.; I2 sublimed onto the solid Ag(P4)2Al(OC(CF3)3)4 at 77 K, then CD2Cl2 condensed onto mixt.; sealed in NMR tube, placed in dry ice/2-propanol bath, activated by ultrasound at -78 °Cfor 10 min); without isolation, detd. by (31)P NMR, (27)Al NMR, (13)C NMR;
参考文献
Krossing; Raabe
Angewandte Chemie - International Edition, 2001 , vol. 40, # 23 p. 4406 - 4409
