Rohrmann; Shonle
Journal of the American Chemical Society, 1944 , vol. 66, p. 1517,1519
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Powell; Murray; Baldwin
Journal of the American Chemical Society, 1933 , vol. 55, p. 1153
in tetrahydrofuran
other Radiation; under N2; THF added to mixt. of Fe complex and I2; heated in microwave reactor (150 W, 10 min, 90°C, max T=96°C, max P=30 psi); solvent evapd.; triturated with hexanes; filtered; residue washed with hexanes; dried in air;
参考文献
Garringer, Sean M.; Hesse, Andrew J.; Magers, John R.; Pugh, Kristapher R.; O'Reilly, Stacy A.; Wilson, Anne M.
Organometallics, 2009 , vol. 28, # 23 p. 6841 - 6844
in toluene
under N2, addn. of I2 soln. to a soln. of W-compound, at -78°C, allowed to warm to -50°C, addn. of MeOH, stirring at room temp. 12 h; vac. evapn., chromy. on silica gel column, a black band (toluene/hexane, 9/1) and a yellow one (CH2Cl2), vac. evapn. of the second fraction , crystn. from toluene/hexane (1/5) at -78°C, elem. anal.;
参考文献
Colomer, Ernest; Corriu, Robert J. P.; Lheureux, Marc
Organometallics, 1989 , vol. 8, p. 2343 - 2348
