in neat (no solvent) finely dispersed Pt is heated with I2 in a closed tube;;
参考文献
Clementi, G.
Nuovo Cimento, 1855 , vol. 2, p. 198 - 198
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Woehler, L.; Mueller, L. v.
Z. Anorg. Chem., 1925 , vol. 149, p. 382 - 386
in benzene addition of a solution of 17.5 g twice sublimed I2 to a solution of 10 g Bi triphenyle in dry benzene;; filtration and washing the precipitate with benzene; removing the benzene in a vacuum desiccator over paraffine shavings;;