1-甲基-1H-吲哚-4-醇合成路线 (共 3 条)
反应条件
hydrogen; palladium on activated carbon in methanol P=2068.65 Torr; 16 h; Product distribution / selectivity;
参考文献
Kemnitzer, William; Drewe, John; Jiang, Songchun; Zhang, Hong; Crogan-Grundy, Candace; Labreque, Denis; Bubenick, Monica; Attardo, Giorgio; Denis, Real; Lamothe, Serge; Gourdeau, Henriette; Tseng, Ben; Kasibhatla, Shailaja; Sui, Xiong Cai
Journal of Medicinal Chemistry, 2008 , vol. 51, # 3 p. 417 - 423
反应条件
1: With boron tribromide in dichloromethane T=20°C; 2: With sodium hydrogencarbonate in dichloromethane; water Product distribution / selectivity;
参考文献
Cytovia, Inc.
Patent: US2006/104998 A1, 2006 ;
Location in patent: Page/Page column 20 ;
US 20060104998 A1
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene T=20°C; Neat (no solvent)Inert atmosphere;
参考文献
Montalban, Antonio Garrido; Baum, Sven M.; Cowell, Justin; McKillop, Alexander
Tetrahedron Letters, 2012 , vol. 53, # 33 p. 4276 - 4279