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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
6-甲基喹喔啉
合成路线
（共 8 条）
919769-95-2
→
反应条件
7556-94-7
6-甲基喹喔啉
反应条件
potassium hydroxide; potassium hexacyanoferrate(III) in ethanol; water T=100°C; 0.666667 h; microwave irradiation;
参考文献
Chilin, Adriana; Marzaro, Giovanni; Zanatta, Samuele; Guiotto, Adriano
Tetrahedron Letters, 2007 , vol. 48, # 18 p. 3229 - 3231
100-97-0
乌洛托品
+
5255-66-3
N-(对甲苯)氨基甲酸乙酯
→
反应条件
7556-94-7
6-甲基喹喔啉
反应条件
1: With trifluoroacetic acid 1 h; Heating; 2: With potassium hydroxide; potassium hexacyanoferrate(III) in ethanol; water 4 h; Heating;
参考文献
Chilin, Adriana; Marzaro, Giovanni; Zanatta, Samuele; Barbieri, Vera; Pastorini, Giovanni; Manzini, Paolo; Guiotto, Adriano
Tetrahedron, 2006 , vol. 62, # 52 p. 12351 - 12356
5255-66-3
N-(对甲苯)氨基甲酸乙酯
→
反应条件
7556-94-7
6-甲基喹喔啉
反应条件
1: 98 percent / TFA / 0.17 h / 110 °C / microwave irradiation 2: 97 percent / K3Fe(CN)6; KOH / H2O; ethanol / 0.67 h / 100 °C / microwave irradiation View Scheme
参考文献
Chilin, Adriana; Marzaro, Giovanni; Zanatta, Samuele; Guiotto, Adriano
Tetrahedron Letters, 2007 , vol. 48, # 18 p. 3229 - 3231
106-49-0
对甲苯胺
→
反应条件
7556-94-7
6-甲基喹喔啉
反应条件
1: 98 percent / TEA / tetrahydrofuran / 1 h / 20 °C 2: 80 percent / trifluoroacetic acid / 1 h / Heating 3: 92 percent / potassium hydroxide / H2O / 2 h / Heating 4: 13 percent / acetic acid / 1 h / Heating View Scheme
参考文献
Chilin, Adriana; Marzaro, Giovanni; Zanatta, Samuele; Barbieri, Vera; Pastorini, Giovanni; Manzini, Paolo; Guiotto, Adriano
Tetrahedron, 2006 , vol. 62, # 52 p. 12351 - 12356
100-97-0
乌洛托品
+
350-96-9
p-甲苯胺三氟乙酰胺
→
反应条件
529-81-7
2,8-DIMETHYL-6H,12H-5,11-METHANODIBENZO[B,F][1,5]DIAZOCINE
+
7556-94-7
6-甲基喹喔啉
反应条件
1: With trifluoroacetic acid 1 h; Heating; 2: With potassium hydroxide; potassium hexacyanoferrate(III) in ethanol; water 4 h; Heating;
参考文献
Chilin, Adriana; Marzaro, Giovanni; Zanatta, Samuele; Barbieri, Vera; Pastorini, Giovanni; Manzini, Paolo; Guiotto, Adriano
Tetrahedron, 2006 , vol. 62, # 52 p. 12351 - 12356
100-97-0
乌洛托品
+
103-89-9
4'-甲基乙酰苯胺
→
反应条件
529-81-7
2,8-DIMETHYL-6H,12H-5,11-METHANODIBENZO[B,F][1,5]DIAZOCINE
+
7556-94-7
6-甲基喹喔啉
反应条件
1: With trifluoroacetic acid 1 h; Heating; 2: With potassium hydroxide; potassium hexacyanoferrate(III) in ethanol; water 4 h; Heating;
参考文献
Chilin, Adriana; Marzaro, Giovanni; Zanatta, Samuele; Barbieri, Vera; Pastorini, Giovanni; Manzini, Paolo; Guiotto, Adriano
Tetrahedron, 2006 , vol. 62, # 52 p. 12351 - 12356
919769-96-3
→
反应条件
反应条件
acetic acid 1 h; Heating;
参考文献
Chilin, Adriana; Marzaro, Giovanni; Zanatta, Samuele; Barbieri, Vera; Pastorini, Giovanni; Manzini, Paolo; Guiotto, Adriano
Tetrahedron, 2006 , vol. 62, # 52 p. 12351 - 12356
7556-94-7
6-甲基喹喔啉
→
反应条件
439811-22-0
6-喹唑啉羧醛
反应条件
selenium(IV) oxide T=160°C; 12 h;
参考文献
Chen, Li; Chen, Shaoqing; Liu, Jin-Jun
Patent: US2006/84804 A1, 2006 ;
Location in patent: Page/Page column 7-8 ;
US 20060084804 A1
