反应条件
1: 90 percent / Jones reagent / acetone / 3 h / -10 °C
2: 96 percent Turnov. / 1,5-diazabicyclo<5.4.0>undec-5-ene / benzene / 18 h / Ambient temperature
3: 93 percent / lithium tri-s-butylborohydride / tetrahydrofuran / 0.5 h / -78 °C
4: 100 percent / pyridinium toluene-p-sulphonate / CH2Cl2 / 4 h / Ambient temperature
5: 90 percent / tetrabutylammonium fluoride / tetrahydrofuran / 5.5 h / 0 °C
6: 93 percent / pyridinium chlorochromate, sodium acetate / CH2Cl2 / 2 h / Ambient temperature
7: 99 percent / H2O, AcOH / tetrahydrofuran / 24 h / Ambient temperature
View Scheme
参考文献
Gill, Melvyn; Rickards, Rodney W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 599 - 606