1,3-丙二醇二甲基丙烯酸酯合成路线 (共 2 条)
反应条件
1: 2-hydroxy-3-propyl methacrylate With 4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=-25°C; Inert atmosphere;
2: methacrylic acid anhydride T=20°C; 20 h; Inert atmosphere;
参考文献
Blanazs, Adam; Madsen, Jeppe; Battaglia, Giuseppe; Ryan, Anthony J.; Armes, Steven P.
Journal of the American Chemical Society, 2011 , vol. 133, # 41 p. 16581 - 16587
反应条件
sulfuric acid; hydroquinone
参考文献
Arbusova,I.A. et al.
J. Appl. Chem. USSR (Engl. Transl.), 1963 , vol. 36, # 8 p. 1833 - 1837,1774 - 1777