3-(苯基甲氧基)-苯丙醛合成路线 （共 13 条）
反应条件
1: 4 Angstroem molecular sieves / CH2Cl2 / 2.5 h / Ambient temperature 2: hydrogen / 1.) PtO2; 2.) Pd/C / 1.) aq. EtOH; 2.) aq. EtOH, 6 h View Scheme
参考文献
Guanti, Giuseppe; Banfi, Luca; Narisano, Enrica; Riva, Renata; Thea, Sergio
Tetrahedron Letters, 1992 , vol. 33, # 27 p. 3919 - 3922
反应条件
pyridinium chlorochromate in dichloromethane
3 h;
参考文献
Aidhen, Indrapal Singh; Narasimhan, N. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1993 , vol. 32, # 2 p. 222 - 228
反应条件
diisobutylaluminium hydride in dichloromethane
T=-78°C; 0.5 h;
参考文献
Guanti, Giuseppe; Banfi, Luca; Narisano, Enrica; Riva, Renata; Thea, Sergio
Tetrahedron Letters, 1992 , vol. 33, # 27 p. 3919 - 3922
Title/Abstract View citing articles Show Details
Guanti, Giuseppe; Banfi, Luca; Riva, Renata
Tetrahedron, 1994 , vol. 50, # 41 p. 11945 - 11966
反应条件
1: H2 / 5percent Pd/C / methanol / 1 h / Ambient temperature
2: LiAlH4 / tetrahydrofuran; diethyl ether / 1 h / Heating
3: (COCl)2, NEt3 / dimethylsulfoxide
View Scheme
参考文献
Hashizume; Ito; Kanaya; Nagashima; Usui; Oshima; Kanao; Tomoda; Sunazuka; Kumagai; Omura
Chemical and Pharmaceutical Bulletin, 1994 , vol. 42, # 6 p. 1272 - 1278
反应条件
1: 97 percent / conc. H2SO4 / 7 h / Heating
2: 98 percent / hydrogen / PtO2 / aq. ethanol / 20 h / Ambient temperature
3: 91 percent / K2CO3 / dimethylformamide / 24 h / 80 °C
4: DIBALH / CH2Cl2 / 0.5 h / -78 °C
View Scheme
参考文献
Guanti, Giuseppe; Banfi, Luca; Riva, Renata
Tetrahedron, 1994 , vol. 50, # 41 p. 11945 - 11966
反应条件
1: 98 percent / hydrogen / PtO2 / aq. ethanol / 20 h / Ambient temperature
2: 91 percent / K2CO3 / dimethylformamide / 24 h / 80 °C
3: DIBALH / CH2Cl2 / 0.5 h / -78 °C
View Scheme
参考文献
Guanti, Giuseppe; Banfi, Luca; Riva, Renata
Tetrahedron, 1994 , vol. 50, # 41 p. 11945 - 11966
反应条件
1: 98 percent / H2 / PtO2 / ethanol / 20 h / Ambient temperature
2: 91 percent / K2CO3 / dimethylformamide / 24 h / 80 °C
3: DIBALH / CH2Cl2 / 0.5 h / -78 °C
View Scheme
参考文献
Guanti, Giuseppe; Banfi, Luca; Narisano, Enrica; Riva, Renata; Thea, Sergio
Tetrahedron Letters, 1992 , vol. 33, # 27 p. 3919 - 3922
反应条件
1: 93 percent / pyridine, piperdine / 8 h / Heating
2: 97 percent / H2SO4 / 7 h / Heating
3: 98 percent / H2 / PtO2 / ethanol / 20 h / Ambient temperature
4: 91 percent / K2CO3 / dimethylformamide / 24 h / 80 °C
5: DIBALH / CH2Cl2 / 0.5 h / -78 °C
View Scheme
参考文献
Guanti, Giuseppe; Banfi, Luca; Narisano, Enrica; Riva, Renata; Thea, Sergio
Tetrahedron Letters, 1992 , vol. 33, # 27 p. 3919 - 3922
反应条件
1: NaOCH3 / CH2Cl2 / Ambient temperature
2: H2 / 5percent Pd/C / methanol / 1 h / Ambient temperature
3: LiAlH4 / diethyl ether / 1 h / Heating
4: 1.) (COCl)2, DMSO, 2.) Et3N / 1.) CH2Cl2, -40 deg C, 25 min, 2.) CH2Cl2, -40 deg C, 5 min
View Scheme
参考文献
Hashizume; Ito; Yamada; Nagashima; Kanao; Tomoda; Sunazuka; Kumagai; Omura
Chemical and pharmaceutical bulletin, 1994 , vol. 42, # 3 p. 512 - 520
反应条件
1: LiAlH4 / tetrahydrofuran; diethyl ether / 1 h / Heating
2: (COCl)2, NEt3 / dimethylsulfoxide
View Scheme
参考文献
Hashizume; Ito; Kanaya; Nagashima; Usui; Oshima; Kanao; Tomoda; Sunazuka; Kumagai; Omura
Chemical and Pharmaceutical Bulletin, 1994 , vol. 42, # 6 p. 1272 - 1278
