1-环丙基-2,2,2-三氟乙烷酮合成路线 (共 3 条)
反应条件
1: With cesium fluoride in neat (no solvent)
T=20°C; Schlenk techniqueInert atmosphere;
2: With tetra-n-butylammonium fluoride trihydrate in neat (no solvent)
T=20°C; 2 h; Schlenk techniqueInert atmosphere;
参考文献
Wang, Yi; Yuan; Xing, Chun-Hui; Lu, Long
Tetrahedron Letters, 2014 , vol. 55, # 5 p. 1045 - 1048
反应条件
lithium bromide in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=160°C; 1 h;
参考文献
Kitamura, Hiroshi; Oshima, Takumi
Organic Letters, 2008 , vol. 10, # 2 p. 293 - 296
参考文献
Science Union et Cie
Patent: US4378366 A1, 1983 ;