(S)-3,3'-二溴-2,2'-二甲氧基-1,1'-联萘合成路线 (共 5 条)
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine; bromine 1) 25 deg C, 3 h, ether-hexane, 2) -78 deg C, ether-hexane-pentane; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 46, # 2 p. 393 - 406
反应条件
boron tribromide in dichloromethane Substitution;
参考文献
Arnold, Leggy A.; Imbos, Rosalinde; Mandoli, Alessandro; De Vries, Andre H.M.; Naasz, Robert; Feringa, Ben L.
Tetrahedron, 2000 , vol. 56, # 18 p. 2865 - 2878
反应条件
sodium hydrogencarbonate; tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether; water Arylation; 16 h; Heating;
参考文献
Arnold, Leggy A.; Imbos, Rosalinde; Mandoli, Alessandro; De Vries, Andre H.M.; Naasz, Robert; Feringa, Ben L.
Tetrahedron, 2000 , vol. 56, # 18 p. 2865 - 2878
反应条件
boron tribromide in dichloromethane Substitution;
参考文献
Arnold, Leggy A.; Imbos, Rosalinde; Mandoli, Alessandro; De Vries, Andre H.M.; Naasz, Robert; Feringa, Ben L.
Tetrahedron, 2000 , vol. 56, # 18 p. 2865 - 2878
反应条件
boron tribromide in dichloromethane Substitution;
参考文献
Arnold, Leggy A.; Imbos, Rosalinde; Mandoli, Alessandro; De Vries, Andre H.M.; Naasz, Robert; Feringa, Ben L.
Tetrahedron, 2000 , vol. 56, # 18 p. 2865 - 2878