反应条件
Stage #1: <a href="#" onclick="return RXDsubstances(event, this, '385888', constants.ctx, '0')">1,3-cylohexanedione</a> <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '506297', constants.ctx, '0')">methanesulfonyl chloride</a>; <a href="#" onclick="return RXDsubstances(event, this, '605283', constants.ctx, '0')">triethylamine</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '741857', constants.ctx, '0')">acetonitrile</a> <br />T=0 - 25°C; 1 h; <br />Stage #2: <a href="#" onclick="return RXDsubstances(event, this, '506523', constants.ctx, '0')">thiophenol</a> <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '605283', constants.ctx, '0')">triethylamine</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '741857', constants.ctx, '0')">acetonitrile</a> <br />T=0 - 25°C; 14 h; <br />
参考文献
Trost, Barry M.; Bream, Robert N.; Xu, Jiayi Angewandte Chemie - International Edition, 2006 , vol. 45, # 19 p. 3109 - 3112