alpha,alpha,2-三甲基苄醇合成路线 （共 27 条）
参考文献
Kay; Perkin
Journal of the Chemical Society, 1905 , vol. 87, p. 1077
反应条件
Destillation ueber P2O5;
参考文献
Eisenlohr; Schulz
Chemische Berichte, 1924 , vol. 57, p. 1819
参考文献
Bergmann; Weizmann
Transactions of the Faraday Society, 1936 , vol. 32, p. 1327,1328 Anm.
参考文献
Ramart; Hoch
Bulletin de la Societe Chimique de France, 1938 , vol. <5> 5, p. 848,860
参考文献
Tiffeneau
Annales de Chimie (Cachan, France), 1907 , vol. <8>10, p. 190
Annales de Chimie (Cachan, France), 1907 , vol. <8>11, p. 144
反应条件
palladium diacetate; caesium carbonate; tri-cyclo-hexyl-phosphine in o-xylene
8 h; Heating;
参考文献
Terao, Yoshito; Wakui, Hiroyuki; Nomoto, Michiyo; Satoh, Tetsuya; Miura, Masahiro; Nomura, Masakatsu
Journal of Organic Chemistry, 2003 , vol. 68, # 13 p. 5236 - 5243
反应条件
1: dihydrogen peroxide; sulfuric acid / diethyl ether; water / 24 h / 0 - 20 °C
2: copper diacetate; 1,10-phenanthroline; triethylamine / toluene; acetonitrile / 1 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Too, Pei Chui; Tnay, Ya Lin; Chiba, Shunsuke
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1217 - 1225
