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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
7578-51-0
合成路线
（共 11 条）
5751-52-0
7-甲氧基-4H-色烯-4-酮
+
133730-34-4
2,4-二甲氧基苯硼酸
→
反应条件
7578-51-0
反应条件
1: 7-methoxy-4H-chromen-4-one With 1,10-phenanthroline; oxygen; palladium diacetate in N,N-dimethyl-formamide Heck type reaction; 0.0833333 h; 2: 2,4-dimethoxybenzeneboronic acid in N,N-dimethyl-formamide T=100°C; Heck type reaction; 24 h; regioselective reaction;
参考文献
Khoobi, Mehdi; Alipour, Masoumeh; Zarei, Samaneh; Jafarpour, Farnaz; Shafiee, Abbas
Chemical Communications, 2012 , vol. 48, # 24 p. 2985 - 2987
132351-64-5
→
反应条件
7578-51-0
反应条件
perchloric acid; thallium(III) nitrate in methanol; chloroform T=25°C;
参考文献
Kinoshita, Takeshi; Ichinose, Koji; Sankawa, Ushio
Tetrahedron Letters, 1990 , vol. 31, # 50 p. 7355 - 7356
132351-64-5
→
反应条件
7578-51-0
反应条件
sulfuric acid; iodine in dimethyl sulfoxide T=100°C; 8 h;
参考文献
Gao, Jin-Ming; Lu, Jia-Wen; Zhang, An-Ling; Cheng, Yong-Xian; Watchueng, Jean; Konishi, Yasuo
Journal of Chemical Research, 2006 , # 3 p. 163 - 164
36685-67-3
→
反应条件
7578-51-0
反应条件
1: H2SO4 / dimethylsulfoxide / 0.17 h / 100 °C 2: 53 mg / I2; H2SO4 / dimethylsulfoxide / 8 h / 100 °C View Scheme
参考文献
Gao, Jin-Ming; Lu, Jia-Wen; Zhang, An-Ling; Cheng, Yong-Xian; Watchueng, Jean; Konishi, Yasuo
Journal of Chemical Research, 2006 , # 3 p. 163 - 164
552-41-0
丹皮酚
→
反应条件
7578-51-0
反应条件
1: 65 percent / aq. KOH / ethanol / 45 h / 0 - 20 °C 2: H2SO4 / dimethylsulfoxide / 0.17 h / 100 °C 3: 53 mg / I2; H2SO4 / dimethylsulfoxide / 8 h / 100 °C View Scheme
参考文献
Gao, Jin-Ming; Lu, Jia-Wen; Zhang, An-Ling; Cheng, Yong-Xian; Watchueng, Jean; Konishi, Yasuo
Journal of Chemical Research, 2006 , # 3 p. 163 - 164
89-84-9
2,4-二羟基苯乙酮
→
反应条件
7578-51-0
反应条件
1: K2CO3 / acetone / Heating 2: 65 percent / aq. KOH / ethanol / 45 h / 0 - 20 °C 3: H2SO4 / dimethylsulfoxide / 0.17 h / 100 °C 4: 53 mg / I2; H2SO4 / dimethylsulfoxide / 8 h / 100 °C View Scheme
参考文献
Gao, Jin-Ming; Lu, Jia-Wen; Zhang, An-Ling; Cheng, Yong-Xian; Watchueng, Jean; Konishi, Yasuo
Journal of Chemical Research, 2006 , # 3 p. 163 - 164
108-46-3
间苯二酚
→
反应条件
7578-51-0
反应条件
1: H2SO4 / Heating 2: K2CO3 / acetone / Heating 3: 65 percent / aq. KOH / ethanol / 45 h / 0 - 20 °C 4: H2SO4 / dimethylsulfoxide / 0.17 h / 100 °C 5: 53 mg / I2; H2SO4 / dimethylsulfoxide / 8 h / 100 °C View Scheme
参考文献
Gao, Jin-Ming; Lu, Jia-Wen; Zhang, An-Ling; Cheng, Yong-Xian; Watchueng, Jean; Konishi, Yasuo
Journal of Chemical Research, 2006 , # 3 p. 163 - 164
73220-33-4
→
反应条件
7578-51-0
反应条件
1.1: hydrogenchloride / dichloromethane; water / 1 h / Reflux 2.1: 1,10-phenanthroline; oxygen; palladium diacetate / N,N-dimethyl-formamide / 0.08 h 2.2: 24 h / 100 °C View Scheme
参考文献
Khoobi, Mehdi; Alipour, Masoumeh; Zarei, Samaneh; Jafarpour, Farnaz; Shafiee, Abbas
Chemical Communications, 2012 , vol. 48, # 24 p. 2985 - 2987
32140-93-5
→
反应条件
7578-51-0
反应条件
phosphoric acid; potassium iodide
参考文献
Spatz; Koral
Journal of Organic Chemistry, 1959 , vol. 24, p. 1381
829-20-9
2,4-二甲氧基苯乙酮
→
反应条件
7578-51-0
反应条件
1: NaNH2; diethyl ether 2: potassium iodide; phosphoric acid View Scheme
参考文献
Spatz; Koral
Journal of Organic Chemistry, 1959 , vol. 24, p. 1381
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