N,N-二甲基硫代甲酰胺合成路线 （共 52 条）
反应条件
lithium diisopropyl amide in tetrahydrofuran
参考文献
Campaigne,E. et al.
Synthetic Communications, 1976 , vol. 6, p. 387 - 397
反应条件
1H-imidazole; methyl iodide in tetrahydrofuran
4 h; Inert atmosphereReflux;
参考文献
Ellwood, Adam R.; Porter, Michael J.
Journal of Organic Chemistry, 2009 , vol. 74, # 20 p. 7982 - 7985
参考文献
Singh, Harjit; Batra, Manohar S.; Singh, Paramjit
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 131 - 136
反应条件
sodium amide in toluene
参考文献
Scott,M.D.; Spedding,H.
Journal of the Chemical Society [Section] C: Organic, 1968 , p. 1603 - 1609
反应条件
(i) LDA, THF, hexane, (ii) /BRN= 505934/; Multistep reaction;
参考文献
Seebach,D. et al.
Chemische Berichte, 1976 , vol. 109, p. 1309 - 1323
反应条件
lithium diisopropyl amide in tetrahydrofuran
参考文献
Campaigne,E. et al.
Synthetic Communications, 1976 , vol. 6, p. 387 - 397
反应条件
1: N,N-dimethyl-thioformamide; phenyllithium in tetrahydrofuran; diethyl ether; cyclohexane
T=-78 - 20°C;
2: Bromure de phenyl magnesium in tetrahydrofuran; diethyl ether; cyclohexane
T=20°C; 2 h;
参考文献
Murai, Toshiaki; Asai, Fumio
Journal of the American Chemical Society, 2007 , vol. 129, # 4 p. 780 - 781
反应条件
1: N,N-dimethyl-thioformamide; phenyllithium in diethyl ether
T=-78 - 20°C; 1 h;
2: dimethyl zinc in diethyl ether
T=0 - 20°C; 6 h;
参考文献
Murai, Toshiaki; Matsushita, Koji
Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 5 p. 1094 - 1103
反应条件
silver trifluoroacetate; triethylamine in acetonitrile
1 h; Ambient temperature;
参考文献
Shibuya, Isao; Taguchi, Yoichi; Tsuchiya, Tohru; Oishi, Akihiro; Katoh, Eisaku
Bulletin of the Chemical Society of Japan, 1994 , vol. 67, # 11 p. 3048 - 3052
反应条件
lithium diisopropyl amide in tetrahydrofuran
-78 deg C, then warm to Rt, over 3 h;
参考文献
Ablenas, F. J.; George, B. E.; Maleki, M.; Jain, R.; Hopkinson, A. C.; Lee-Ruff, E.
Canadian Journal of Chemistry, 1987 , vol. 65, p. 1800 - 1803
