1-(5-乙炔基-2-甲基-4,5-二氢-3-呋喃基)乙酮合成路线 （共 3 条）
反应条件
copper diacetate; manganese triacetate in acetic acid
T=75°C; 0.5 h;
参考文献
Melikyan, G. G.; Mkrtchyan, D. A.; Badanyan, Sh. O.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1980 , vol. 16, # 7 p. 678 - 680
Khimiya Geterotsiklicheskikh Soedinenii, 1980 , # 7 p. 884 - 887
反应条件
copper diacetate; manganese triacetate in acetic acid
8 equiv acetoacetic acid methyl ester, 4 equiv Mn(OAc)3, 1 equiv Cu(OAc)2, 30°C, 30 min; chromy. (silica);
参考文献
Melikyan, Gagik G.; Vostrowsky, Otto; Bauer, Walter; Bestmann, Hans Juergen
Journal of Organometallic Chemistry, 1992 , vol. 423, # 1 p. C24 - C27
反应条件
manganese triacetate
1.) acetic acid, 2.) acetic acid, 45 deg C, 6 h; Multistep reaction;
参考文献
Melikyan, Gagik G.; Vostrowsky, Otto; Bauer, Walter; Bestmann, Hans Juergen
Journal of Organometallic Chemistry, 1992 , vol. 423, # 1 p. C24 - C27
