5,5,6,6,7,7,8,8,9,9,9-Undeca氟壬烷-2,4-二酮合成路线 （共 4 条）
→
75824-01-05,5,6,6,7,7,8,8,9,9,9-Undeca氟壬烷-2,4-二酮
反应条件
sodium hydride in diethyl ether
参考文献
Peglion, Jean-Louis; Pastor, Raphael-Emile; Cambon, Aime-Roger
Bulletin de la Societe Chimique de France, 1980 , vol. 2, # 5-6 p. 309 - 315
→
75824-01-05,5,6,6,7,7,8,8,9,9,9-Undeca氟壬烷-2,4-二酮
反应条件
1: 82 percent / NH3 / diethyl ether / 1 h / Ambient temperature 2: 78 percent / aq. HCl / 1 h / Heating View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 80, # 1 p. 9 - 12
→
75824-01-05,5,6,6,7,7,8,8,9,9,9-Undeca氟壬烷-2,4-二酮
反应条件
1: 94 percent / acetonitrile / 20 h / 70 °C 2: 90 percent / HCl / methanol; H2O / 2 h / Heating View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 34, p. 265
→
75824-01-05,5,6,6,7,7,8,8,9,9,9-Undeca氟壬烷-2,4-二酮
反应条件
1: sodium dithionite, sodium bicarbonate / acetonitrile; H2O / 40 °C 2: acetonitrile; H2O / 2 h / Ambient temperature 3: 4 N aq. HCl / acetonitrile; H2O / 0.5 h / Ambient temperature View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 59, # 2 p. 179 - 183
