1-叔丁基-7-噁双环[4.1.0]庚烷合成路线 (共 14 条)
反应条件
1: 42 percent / trichloroacetic acid / CH2Cl2 / 0.33 h / 25 °C
2: 0.2 N H2SO4 / 0.08 h / Ambient temperature
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参考文献
Corona, Tiberio; Crotti, Paolo; Macchia, Franco; Ferretti, Maria
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 377 - 379
反应条件
toluene-4-sulfonic acid in dichloromethane
T=25°C; 0.25 h; Further byproducts given;
参考文献
Corona, Tiberio; Crotti, Paolo; Ferretti, Maria; Macchia, Franco
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1607 - 1616
反应条件
sulfuric acid
0.25 h; Ambient temperatureor p-TsOH in CH2Cl2;
参考文献
Corona, Tiberio; Crotti, Paolo; Macchia, Franco; Ferretti, Maria
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 377 - 379
反应条件
methanol; toluene-4-sulfonic acid in dichloromethane
0.25 h; Ambient temperature; Further byproducts given;
参考文献
Corona, Tiberio; Crotti, Paolo; Ferretti, Maria; Macchia, Franco
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1607 - 1616