反应条件
1.1: n-BuLi / tetrahydrofuran / 0.5 h / 0 °C
1.2: 37 percent / tetrahydrofuran / 0 - 20 °C
2.1: potassium tert-butoxide / tetrahydrofuran / 0.67 h / 0 °C
2.2: 87 percent / tetra-n-butylammonium iodide / tetrahydrofuran / 8 h / 20 °C
3.1: 86 percent / sodium amalgam; disodium hydrogen phosphate / methanol / 2 h / 20 °C
View Scheme
参考文献
White, James D.; Blakemore, Paul R.; Milicevic, Selena; Choudhry, Satish C.; Cupano, Joseph; Serico, Lucia
Organic Letters, 2002 , vol. 4, # 10 p. 1803 - 1806
