反应条件
1: 1.) Mg, 2.) dilithium tetrachlorocuprate / 1) THF, 2.) THF, -10 deg C, 4 h 2: 1.) NaBH4, Hg(OAc)2, 2.) aq. H2O2, aq. NaOH / 1) THF, 16 h, room temperature; 2) THF, 70 deg C, 1 h 3: 84 percent / pyridinium chlorochromate / CH2Cl2 / 2 h View Scheme
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 59, # 3 p. 721 - 724
