反应条件
sodium tetrahydroborate; oxalyl dichloride; N,N-dimethyl-formamide
1.) acetonitrile, THF, -30 deg C, 1 h, 2.) acetonitrile, THF, from - 30 deg C to RT, 3 h; Yield given. Multistep reaction;
参考文献
Sutherland; Willis
Journal of Labelled Compounds and Radiopharmaceuticals, 1996 , vol. 38, # 1 p. 95 - 102