758640-21-0合成路线 (共 138 条)
参考文献
Beckmann; Fellrath
Justus Liebigs Annalen der Chemie, 1893 , vol. 273, p. 28
反应条件
1: 6 percent Spectr. / t-butyl hydroperoxide (TBHP) / cobalt(II) schiff base complex CoII(L1) / dimethylsulfoxide / 8 h / 40 °C 2: 97 percent Spectr. / t-butyl hydroperoxide (TBHP) / cobalt(II) schiff base complex CoII(L1) / dimethylsulfoxide / 8 h / 40 °C View Scheme
参考文献
Maruyama, Kazushige; Kusukawa, Takahiro; Higuchi, Yoshihiko; Nishinaga, Akira
Chemistry Letters, 1991 , # 7 p. 1093 - 1096
反应条件
trichlorophosphate T=90°C; 1 h;
参考文献
Kappe, Thomas; Aigner, Rudolf; Hohengassner, Peter; Stadlbauer, Wolfgang
Journal fuer Praktische Chemie/Chemiker-Zeitung, 1994 , vol. 336, # 7 p. 596 - 601
反应条件
copper diacetate; palladium diacetate; potassium iodide in acetonitrile T=60°C; P=760.051 Torr; regioselective reaction;
参考文献
Guan, Zheng-Hui; Chen, Ming; Ren, Zhi-Hui
Journal of the American Chemical Society, 2012 , vol. 134, # 42 p. 17490 - 17493,4
反应条件
2,2,6,6-tetramethylpiperidinyl-lithium in tetrahydrofuran; pentane T=25°C; 24 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 14, # 23 p. 5964 - 5967
反应条件
1: With sodium t-butanolate in toluene T=80°C; 0.5 h; 2: With bis[2-(diphenylphosphino)phenyl] ether; palladium diacetate in toluene T=80°C; 18 h;
参考文献
Ishibashi, Koichi; Tsue, Hirohito; Tokita, Satoshi; Matsui, Kazuhiro; Takahashi, Hiroki; Tamura, Rui
Organic Letters, 2006 , vol. 8, # 26 p. 5991 - 5994
反应条件
tert.-butylhydroperoxide; 3 A molecular sieve; zirconium tetra-t-butoxide in dichloromethane 5 h; Heating;
参考文献
Krohn, Karsten; Kuepke, Jochen
Journal fuer Praktische Chemie - Practical Applications and Applied Chemistry (Germany), 1999 , vol. 341, # 5 p. 509 - 511
反应条件
dihydrogen peroxide; PCWP in chloroform T=40°C; 2.5 h; Further byproducts given;
参考文献
Tetrahedron, , vol. 48, # 40 p. 8677 - 8684
反应条件
potassium superoxide; 18-crown-6 ether in benzene T=25°C; 72 h; other solvent; MechanismProduct distribution;
参考文献
Frimer, Aryeh A.; Aljadeff, Gladis; Ziv, Joseph
Journal of Organic Chemistry, 1983 , vol. 48, # 10 p. 1700 - 1705
参考文献
Huebner
Chemische Berichte, 1902 , vol. 35, p. 731