758640-21-0合成路线 （共 138 条）
反应条件
oxygen in acetonitrile T=80°C; P=3750.38 Torr; 3 h; AutoclaveIrradiation;
参考文献
Su, Fangzheng; Mathew, Smitha C.; Moehlmann, Lennart; Antonietti, Markus; Wang, Xinchen; Blechert, Siegfried
Angewandte Chemie - International Edition, 2011 , vol. 50, # 3 p. 657 - 660
反应条件
iodine; tert-butylamine in acetonitrile 6 h; Heating;
参考文献
Journal of Chemical Research, Miniprint, , # 1 p. 311 - 332
反应条件
iodine in acetonitrile 6 h; Heating; Title compound not separated from byproducts;
参考文献
Journal of Chemical Research, Miniprint, , # 1 p. 311 - 332
反应条件
oxalyl dichloride; dimethyl sulfoxide 1.) CH2Cl2, -60 deg C, 3 min; 2.) CH2Cl2, -60 deg C, 10 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Keirs, David; Overton, Karl
Journal of the Chemical Society, Chemical Communications, 1987 , p. 1660 - 1661
反应条件
oxalyl dichloride 1.) CH2Cl2, -60 deg C, 3 min; 2.) CH2Cl2, -60 deg C, 10 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Keirs, David; Overton, Karl
Journal of the Chemical Society, Chemical Communications, 1987 , p. 1660 - 1661
反应条件
potassium hydroxide; potassium hexacyanoferrate(III) in water 42 h; Heating; Product distribution;
参考文献
Barbiero, Gennaro; Kim, Whan-Gi; Hay, Allan S.
Tetrahedron Letters, 1994 , vol. 35, # 34 p. 6199 - 6202
反应条件
NiCuFeO(x) in anhydrous xylene 12 h; Inert atmosphereSealed tubeReflux;
参考文献
Cui, Xinjiang; Dai, Xingchao; Deng, Youquan; Shi, Feng
Chemistry - A European Journal, 2013 , vol. 19, # 11 p. 3665 - 3675
反应条件
vanadyl acetylacetonate; PhIO2 in benzene Heating; Product distribution;
参考文献
Pharmazie, , vol. 42, # 2 p. 132 - 132
参考文献
Postowsky; Lugowkin
Journal fuer Praktische Chemie (Leipzig), 1929 , vol. <2> 122, p. 145
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1929 , vol. 61, p. 1283
反应条件
1: hydrogenchloride / acetonitrile; water / 0 °C 2: [Cp*Rh(OAc)2] / methanol / 90 °C / |Sealed tube 3: oxygen; potassium tert-butylate / dimethyl sulfoxide / 5 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 15, # 20 p. 5294 - 5297
