758640-21-0合成路线 （共 138 条）
反应条件
methanesulfonic acid; hydrogen; [Ru(acac)3]; 1,1,1-tris (diphenylphosphinomethyl)ethane in tetrahydrofuran T=140°C; 24 h; AutoclaveInert atmosphere;
参考文献
Li, Yuehui; Sorribes, Ivan; Yan, Tao; Junge, Kathrin; Beller, Matthias
Angewandte Chemie - International Edition, 2013 , vol. 52, # 46 p. 12156 - 12160
Angew. Chem., 2013 , vol. 125, # 46 p. 12378 - 12382,5
反应条件
1: With hydrogenchloride in methanol T=20°C; 2: With N-methylpiperidine zinc borohydride in methanol T=20°C; 0.75 h;
参考文献
Alinezhad, Heshmatollah; Tajbakhsh, Mahmood; Zamani, Reza
Synthetic Communications, 2006 , vol. 36, # 23 p. 3609 - 3615
反应条件
in n-heptane; ethyl acetate; N,N-dimethyl-formamide; mineral oil
参考文献
Abbott Laboratories
Patent: US6921763 B2, 2005 ;
反应条件
lithium aluminium tetrahydride 1.) nitrosation, 2.) ether, reflux; Multistep reaction;
参考文献
Antrick
Justus Liebigs Annalen der Chemie, 1885 , vol. 227, p. 372
反应条件
dihydrogen peroxide; PCWP in chloroform T=40°C; 2.5 h; Further byproducts given;
参考文献
Tetrahedron, , vol. 48, # 40 p. 8677 - 8684
参考文献
Huebner
Chemische Berichte, 1902 , vol. 35, p. 731
参考文献
Mailhe
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1921 , vol. 172, p. 281
Bulletin de la Societe Chimique de France, 1921 , vol. <4>29, p. 107
反应条件
RuCl2(PPh3)2 in 1,4-dioxane T=180°C; 5 h;
参考文献
Shim; Youn; Lee; Kim; Cho; Uemura; Watanabe
Synthetic Communications, 1996 , vol. 26, # 7 p. 1349 - 1353
反应条件
1: 1.) SnCl4, Bu3N, 2.) KOH, H2O / 1.) chlorobenzene, -50 deg C to 80 deg C, 2.) chlorobenzene, THF, reflux 2: 80 percent / quinone, LiCl / PdCl2(MeCN)2 / tetrahydrofuran / 18 h / Heating View Scheme
参考文献
Tanabe Seiyaku Co., Ltd.
Patent: US4443615 A1, 1984 ;
反应条件
Neobead P (Al2O3:SiO2:Na2O=88:9:3) T=300°C; P=760 Torr;
参考文献
Nishida, Takuo; Tokuda, Yoshikazu; Tsuchiya, Michihiro
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1995 , # 4 p. 823 - 830
