758640-21-0合成路线 (共 138 条)
参考文献
Journal of the Chemical Society, , p. 1119,1124
反应条件
1: 4-(N,N-dimethlyamino)pyridine; diisopropyl-carbodiimide / dichloromethane / 24 h / 0 - 23 °C / Inert atmosphere 2: silver trifluoroacetate / dichloromethane / 20 h / -78 - 23 °C / Inert atmosphere View Scheme
参考文献
Lai, Ping-Shan; Dubland, Joshua A.; Sarwar, Mohammed G.; Chudzinski, Michael G.; Taylor, Mark S.
Tetrahedron, 2011 , vol. 67, # 39 p. 7586 - 7592
反应条件
1: 3-CPBA / acetone / 0 - 5 °C 2: LiAlH4 / diethyl ether; diethyl ether / 0.33 h View Scheme
参考文献
Gorrod, John W.; Gooderham, Nigel J.
Archiv der Pharmazie (Weinheim, Germany), 1986 , vol. 319, # 3 p. 261 - 265
参考文献
Werner
Chem. News J. Ind. Sci., 1892 , vol. 65, p. 249
反应条件
sulfuric acid; nitric acid
参考文献
Reilly; Moore; Drumm
Journal of the Chemical Society, 1928 , p. 564
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van den Berg
Recueil des Travaux Chimiques des Pays-Bas, 1936 , vol. 55, p. 841,844
反应条件
in acetone T=100°C; 5 h;
参考文献
Take; Okumura; Tsubaki; Terai; Shiokawa
Chemical and Pharmaceutical Bulletin, 1993 , vol. 41, # 3 p. 507 - 515
反应条件
hydrogenchloride; ethanol; water
参考文献
Turner; Djerassi
Journal of the American Chemical Society, 1950 , vol. 72, p. 3081
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; potassium carbonate; sodium iodide T=100°C; 0.75 h; Product distribution; Further Variations:Reagents;
参考文献
Dash; Kudav; Parihar
Journal of Heterocyclic Chemistry, 2006 , vol. 43, # 2 p. 401 - 404
反应条件
tert.-butylhydroperoxide; cobalt(II) schiff base complex CoII(L1) in dimethyl sulfoxide T=40°C; 8 h;
参考文献
Maruyama, Kazushige; Kusukawa, Takahiro; Higuchi, Yoshihiko; Nishinaga, Akira
Chemistry Letters, 1991 , # 7 p. 1093 - 1096
反应条件
tert.-butylhydroperoxide; sodium acetate; tetra-(n-butyl)ammonium iodide in water; acetonitrile T=90°C; 8 h;
参考文献
Zhang, Jie; Jiang, Jiewen; Li, Yuling; Zhao, Yun; Wan, Xiaobing
Organic Letters, 2013 , vol. 15, # 13 p. 3222 - 3225