758640-21-0合成路线 （共 138 条）
反应条件
tert.-butylhydroperoxide; Cl2Ru*(x)H2O; 2-oxo-3,3-dimethyl-butanoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone in decane; dimethyl sulfoxide T=50°C; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Wu, Wenliang; Su, Weiping
Journal of the American Chemical Society, 2011 , vol. 133, # 31 p. 11924 - 11927
反应条件
(NH4)2S2O8 in 1,1-dimethylpropan-1-ol T=120°C; 24 h; Inert atmosphereSchlenk techniqueSealed tubeGreen chemistry; stereoselective reaction;
参考文献
Wei, Yu; Tang, Jinghua; Cong, Xuefeng; Zeng, Xiaoming
Green Chemistry, 2013 , vol. 15, # 11 p. 3165 - 3169
参考文献
Ogata,Y.; Nagura,K.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1974 , p. 1089 - 1093
反应条件
1: 40 percent / acetonitrile / 0.5 h / 20 °C 2: 56 percent / 600 °C / 0 - 0.01 Torr View Scheme
参考文献
McNab, Hamish; Monahan, Lilian C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 863 - 868
反应条件
1: 6 percent Spectr. / t-butyl hydroperoxide (TBHP) / cobalt(II) schiff base complex CoII(L1) / dimethylsulfoxide / 8 h / 40 °C 2: 3 percent Spectr. / t-butyl hydroperoxide (TBHP) / cobalt(II) schiff base complex CoII(L1) / dimethylsulfoxide / 8 h / 40 °C View Scheme
参考文献
Maruyama, Kazushige; Kusukawa, Takahiro; Higuchi, Yoshihiko; Nishinaga, Akira
Chemistry Letters, 1991 , # 7 p. 1093 - 1096
反应条件
sulfuric acid; nitric acid
参考文献
Reilly; Moore; Drumm
Journal of the Chemical Society, 1928 , p. 564
Full Text Show Details
van den Berg
Recueil des Travaux Chimiques des Pays-Bas, 1936 , vol. 55, p. 841,844
反应条件
sulfuric acid; nitric acid
T=0°C;
参考文献
Reilly; Moore; Drumm
Journal of the Chemical Society, 1928 , p. 564
反应条件
1: 56 percent / quinoline, sodium carbonate / 2-methoxy-ethanol / 0.75 h / Heating
2: acetic acid / 1 h / Heating
View Scheme
参考文献
El-Hamamy, Ahmad A.; Hill, John; Townend, John
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 573 - 580
参考文献
Kotschetkow et al.
Zhurnal Obshchei Khimii, 1956 , vol. 26, p. 3144,3147; engl. Ausg. S. 3505, 3507
反应条件
NiCuFeO(x) in anhydrous xylene
12 h; Inert atmosphereSealed tubeReflux;
参考文献
Cui, Xinjiang; Dai, Xingchao; Deng, Youquan; Shi, Feng
Chemistry - A European Journal, 2013 , vol. 19, # 11 p. 3665 - 3675
