2-[(三甲基硅烷基)乙炔基]吡啶合成路线 (共 5 条)
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); diisopropylamine in tetrahydrofuran
T=50°C; 6 h; Inert atmosphere;
参考文献
Wang, Shuai; Cuesta-Seijo, Jose A.; Lafont, Dominique; Palcic, Monica M.; Vidal, Sebastien
Chemistry - A European Journal, 2013 , vol. 19, # 45 p. 15346 - 15357
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran
Heating;
参考文献
Pena, Miguel A.; Perez, Ignacio; Perez Sestelo, Jose; Sarandeses, Luis A.
Chemical Communications, 2002 , # 19 p. 2246 - 2247
反应条件
tris(dibenzylideneacetone)dipalladium (0); triethylamine; triphenylphosphine; copper(l) iodide
T=80°C; 42 h;
参考文献
Heemstra, Jennifer M.; Moore, Jeffrey S.
Organic Letters, 2004 , vol. 6, # 5 p. 659 - 662
反应条件
copper(l) iodide; diisopropylamine; bis-triphenylphosphine-palladium(II) chloride
Sonogashira coupling; 1 h; Heating;
参考文献
Dana, Bogdan H; Robinson, Brian H; Simpson, Jim
Journal of Organometalic Chemistry, 2002 , vol. 648, # 1-2 p. 251 - 269
反应条件
potassium carbonate in tetrahydrofuran; methanol
参考文献
Brunet, Ernesto; Juanes, Olga; Jimenez, Laura; Rodriguez-Ubis, Juan Carlos
Tetrahedron Letters, 2009 , vol. 50, # 38 p. 5361 - 5363