2-(4-溴苯基)-2-重氮基乙酸乙酯合成路线 (共 4 条)
反应条件
tetrabutylammomium bromide; 1,8-diazabicyclo[5.4.0]undec-7-ene; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=45°C; 5 h;
参考文献
Peng, Cheng; Cheng, Jiajia; Wang, Jianbo
Journal of the American Chemical Society, 2007 , vol. 129, # 28 p. 8708 - 8709
反应条件
p-acetamidebenzesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile T=0°C; Inert atmosphere;
参考文献
Fraile, Jose M.; Le Jeune, Karel; Mayoral, Jose A.; Ravasio, Nicoletta; Zaccheria, Federica
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 26 p. 4327 - 4332
反应条件
1: With benzoic acid; hydrazine in tetrahydrofuran T=20°C; 16 h; 2: With N-iodo-N-potassio-p-toluenesulphonamide; potassium hydroxide in tetrahydrofuran; water T=20°C;
参考文献
Nicolle, Simon M.; Moody, Christopher J.
Chemistry - A European Journal, 2014 , vol. 20, # 15 p. 4420 - 4425
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile 0.5 h; Inert atmosphere;
参考文献
Beyzavi, M. Hassan; Nietzold, Carolin; Reissig, Hans-Ulrich; Wiehe, Arno
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 7 p. 1409 - 1422