1-(1-金刚烷)-4,4,4-三氟-1,3-丁二酮合成路线 （共 2 条）
反应条件
1: adamantan-1-yl-ethan-1-one With lithium hexamethyldisilazane in tetrahydrofuran
T=0 - 20°C; 0.333333 h;
2: TFETFA in tetrahydrofuran
T=20°C; 0.333333 h;
3: With ammonium chloride in tetrahydrofuran; water
参考文献
Riofski, Mark V.; John, Jinu P.; Zheng, Mary M.; Kirshner, Julia; Colby, David A.
Journal of Organic Chemistry, 2011 , vol. 76, # 10 p. 3676 - 3683
反应条件
sodium hydride in diethyl ether
12 h; Inert atmosphere;
参考文献
Khamylov; Pochekutova; Petrov; Sizov; Fukin; Kurskii; Arapova
Russian Journal of General Chemistry, 2009 , vol. 79, # 1 p. 31 - 36
