反应条件
Et3N in benzene byproducts: Et3N*HCl; hot soln. of ligand in C6H6 was added dropwise with stirring to hot soln. of Sn compd. in C6H6; mixt. was refluxed for 2 h; Et3N was added; refluxed for 1.5 h; cooled to room temp.; filtered; volatiles removed and dried (vac.); extd. (hexane); hot filtered; evapd.; recrystd. (C6H6/hexane, 1/1); slowly evapd.; elem. anal.;
参考文献
Basu Baul, Tushar S.; Mizar, Archana; Lycka, Antonin; Rivarola, Eleonora; Jirasko, Robert; Holcapek, Michal; de Vos, Dick; Englert, Ulli
Journal of Organometallic Chemistry, 2006 , vol. 691, # 16 p. 3416 - 3425
