3,6-二丁氧基-1,2-苯二甲腈合成路线 （共 7 条）
反应条件
lithium in butan-1-ol 1 h; Heating; Further byproducts given;
参考文献
Aoudia, Mohamed; Cheng, Gongzhen; Kennedy, Vance O.; Kenney, Malcolm E.; Rodgers, Michael A. J.
Journal of the American Chemical Society, 1997 , vol. 119, # 26 p. 6029 - 6039
反应条件
lithium; 1,4-dibutoxy-2,3-naphthalenedicarbonitrile in butan-1-ol 1 h; Heating; Further byproducts given;
参考文献
Aoudia, Mohamed; Cheng, Gongzhen; Kennedy, Vance O.; Kenney, Malcolm E.; Rodgers, Michael A. J.
Journal of the American Chemical Society, 1997 , vol. 119, # 26 p. 6029 - 6039
反应条件
lithium in pentan-1-ol 14 h; Heating;
参考文献
Isosomppi, Marja; Tkachenko, Nikolai V.; Efimov, Alexander; Vahasalo, Heidi; Jukola, Johanna; Vainiotalo, Pirjo; Lemmetyinen, Helge
Chemical Physics Letters, 2006 , vol. 430, # 1-3 p. 36 - 40
反应条件
lithium in pentan-1-ol 12 h; RefluxInert atmosphere;
参考文献
Alekseev; Tkachenko; Efimov; Lemmetyinen
Russian Journal of Physical Chemistry A, 2010 , vol. 84, # 7 p. 1230 - 1241
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=80 - 90°C; 20 h;
参考文献
Gao, Detao; Xu, Haitao; Van Tiantang; Peng, Bixian
Journal of the Chinese Chemical Society, 2001 , vol. 48, # 6 B p. 1189 - 1196
反应条件
potassium carbonate in acetone
60 h; Heating;
参考文献
Cook, Michael J.; Dunn, Adrian J.; Howe, Steven D.; Thomson, Andrew J.; Harrison, Kenneth J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2453 - 2458
反应条件
1: 73 percent / H2SO4 / ethanol; H2O / 3 h / 20 °C
2: 86.4 percent / K2CO3 / dimethylformamide / 20 h / 80 - 90 °C
View Scheme
参考文献
Gao, Detao; Xu, Haitao; Van Tiantang; Peng, Bixian
Journal of the Chinese Chemical Society, 2001 , vol. 48, # 6 B p. 1189 - 1196
