3-(2-萘基氧基)-1-丙醇合成路线 (共 22 条)
反应条件
potassium carbonate; potassium iodide in N,N-dimethyl-formamide
T=70°C; 24 h; Inert atmosphere;
参考文献
Sakai, Fuji; Ji, Zhong-Wei; Liu, Jiang-Hua; Chen, Guo-Song; Jiang, Ming
Chinese Chemical Letters, 2013 , vol. 24, # 7 p. 568 - 572
反应条件
tetrabutyl ammonium fluoride in acetonitrile
T=60°C; 1.5 h;
参考文献
Dong, Wook Kim; Jeong, Hwan-Jeong; Seok, Tae Lim; Sohn, Myung-Hee; Katzenellenbogen, John A.; Dae, Yoon Chi
Journal of Organic Chemistry, 2008 , vol. 73, # 3 p. 957 - 962
反应条件
tetrabutyl ammonium fluoride; water in N,N-dimethyl-formamide
T=70°C; 1 h;
参考文献
Kim, Dong Wook; Jeong, Hwan-Jeong; Lim, Seok Tae; Sohn, Myung-Hee
Angewandte Chemie - International Edition, 2008 , vol. 47, # 44 p. 8404 - 8406
反应条件
potassium fluoride; water; 1-n-butyl-3-methylimidazolium tetrafluoroborate in acetonitrile
T=110°C; 24 h;
参考文献
Kim, Dong Wook; Song, Choong Eui; Chi, Dae Yoon
Journal of the American Chemical Society, 2002 , vol. 124, # 35 p. 10278 - 10279
反应条件
TBAF(tert-BuOH)4 in acetonitrile
T=70°C; 0.5 h;
参考文献
Kim, Dong Wook; Jeong, Hwan-Jeong; Lim, Seok Tae; Sohn, Myung-Hee
Angewandte Chemie - International Edition, 2008 , vol. 47, # 44 p. 8404 - 8406
反应条件
tetrabutyl ammonium fluoride; water in acetonitrile
T=70°C; 1 h;
参考文献
Kim, Dong Wook; Jeong, Hwan-Jeong; Lim, Seok Tae; Sohn, Myung-Hee
Angewandte Chemie - International Edition, 2008 , vol. 47, # 44 p. 8404 - 8406
反应条件
1: β-naphthol With sodium hydroxide
2: 3-bromopropan-1-ol in water
T=20°C;
参考文献
Shi, Zhangjie; He, Chuan
Journal of the American Chemical Society, 2004 , vol. 126, # 42 p. 13596 - 13597
反应条件
potassium fluoride; tetraethylene glycol
T=80°C; 5 h;
参考文献
Yan, Hailong; Oh, Joong-Suk; Song, Choong Eui
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 23 p. 8119 - 8121
反应条件
tetrabutyl ammonium fluoride
T=80°C; 1 h; Product distribution / selectivity;
参考文献
FUTURECHEM CO., LTD.; MOON, Dae Hyuk
Patent: WO2006/65038 A1, 2006 ;
Location in patent: Page/Page column 11-14 ;
反应条件
N,N,N',N'-tetramethyl-7,8-dihydro-6H-dipyrido[1,2-a;2',1'-c][1,4] diazepine-2,12-diamine in N,N-dimethyl-formamide; mineral oil
T=20°C; Inert atmosphere;
参考文献
Sword, Ryan; Baldwin, Luke A.; Murphy, John A.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 9 p. 3560 - 3570